1-甲基-3-苯基丙胺合成路线 （共 111 条）
反应条件
immobilized alkaline protease in 3-methyl pentan-3-ol T=21°C; 0.166667 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Bottalla, Anne-Lise; Queyroy, Severine; Azzi-Schue, Nadia; Vanthuyne, Nicolas; Gastaldi, Stephane; Bertrand, Michele P.; Gil, Gerard
Tetrahedron Asymmetry, 2009 , vol. 20, # 24 p. 2823 - 2834
反应条件
immobilized alkaline protease in 3-methyl pentan-3-ol T=21°C; 3 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Bottalla, Anne-Lise; Queyroy, Severine; Azzi-Schue, Nadia; Vanthuyne, Nicolas; Gastaldi, Stephane; Bertrand, Michele P.; Gil, Gerard
Tetrahedron Asymmetry, 2009 , vol. 20, # 24 p. 2823 - 2834
反应条件
Candida antarctica lipase B T=28°C; 4 h;
参考文献
Gonzalez-Sabin, Javier; Gotor, Vicente; Rebolledo, Francisca
Tetrahedron Asymmetry, 2002 , vol. 13, # 12 p. 1315 - 1320
反应条件
Candida antarctica lipase B Title compound not separated from byproducts;
参考文献
Escoubet, Stephanie; Gastaldi, Stephane; Vanthuyne, Nicolas; Gil, Gerard; Siri, Didier; Bertrand, Michele P.
Journal of Organic Chemistry, 2006 , vol. 71, # 19 p. 7288 - 7292
反应条件
potassium hydroxide in diethylene glycol T=210°C; 8 h;
参考文献
Rahman, S. M. Abdur; Ohno, Hiroaki; Tanaka, Tetsuaki
Tetrahedron Letters, 2001 , vol. 42, # 45 p. 8007 - 8010
反应条件
pyridoxal 5'-phosphate in aq. phosphate buffer; dimethyl sulfoxide T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Paeivioe, Mari; Kanerva, Liisa T.
Process Biochemistry, 2013 , vol. 48, # 10 p. 1488 - 1494
反应条件
pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. phosphate buffer T=37°C; pH=7.4; 0.0833333 h; Enzymatic reaction; enantioselective reaction;
参考文献
Jiang, Jinju; Chen, Xi; Feng, Jinhui; Wu, Qiaqing; Zhu, Dunming
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 100, p. 32 - 39
反应条件
pyridoxal 5'-phosphate; recombinant ω-transaminase from Burkholderia vietnamiensis G4 in aq. buffer T=37°C; pH=7.4; 12 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 100, p. 32 - 39
反应条件
Vibrio fluvialis JS17; 2-oxo-propionic acid in phosphate buffer T=37°C; pH=7.0; Microbiological reaction; Enzyme kinetics; Further Variations:Reagents;
参考文献
Bioscience, Biotechnology and Biochemistry, , vol. 65, # 8 p. 1782 - 1788
反应条件
Alkaline protease in 3-methyl pentan-3-ol T=20°C; 3 h; Enzymatic reaction; optical yield given as percent ee;
参考文献
Organic and Biomolecular Chemistry, , vol. 6, # 21 p. 3917 - 3920
