反应条件
1: 87 percent / LiI / dimethylformamide / 0.83 h / 150 °C
2: 1.) Et33N, NaI, trimethylsilyl chloride, 2.) HgCl2, hexamethyldisilazane, 3.) NaI, aq. HCl / 1) CH3CN, rt, 45 min; 2) CH2Cl2, THF, rt, 120 min; 3) CH2Cl2, THF, 0 deg C, 15 h
View Scheme
参考文献
Hashizume, Yoshinobu; Maki, Shojiro; Ohashi, Mamoru; Niwa, Haruki
Synthetic Communications, 1999 , vol. 29, # 7 p. 1223 - 1233
