2-(烯丙基硫基)-1,3-苯并噻唑合成路线 （共 19 条）
反应条件
sodium hydroxide; Amberlite IRA-400 chloride form in water; acetone
参考文献
Dalal; Pawar; Mahulikar
Organic Preparations and Procedures International, 2005 , vol. 37, # 6 p. 539 - 546
反应条件
in N,N-dimethyl-formamide
T=20°C;
参考文献
Korotkikh, N. I.; Aslanov, A. F.; Shvaika, O. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 6 p. 716 - 717
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 6 p. 855 - 856
反应条件
sodium hydroxide
T=20°C; 16 h;
参考文献
Khodair, Ahmed I.; Al-Masoudi, Najim A.; Gesson, Jean-Pierre
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 11 p. 2061 - 2076
反应条件
in 1,4-dioxane
T=20°C; 0.0833333 h;
参考文献
Yu, Yanfei; Li, Zhengning; Jiang, Lan
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 5 p. 632 - 640
反应条件
potassium hydroxide
T=40 - 45°C; 3 h;
参考文献
Voinova, V. K.; Ostankova, T. V.; Konovalenko, N. A.; Shatalov, G. V.
J. Appl. Chem. USSR (Engl. Transl.), 1990 , vol. 63, # 5 p. 1194 - 1197,1096 - 1098
参考文献
Moore; Waight
Journal of the Chemical Society, 1952 , p. 4237,4240, 4242, 4248, 4249
参考文献
Takahashi; Okada
Yakugaku Zasshi, 1951 , vol. 71, p. 902,904
Chem.Abstr., 1952 , p. 8091
反应条件
1: 52 percent / Br2; acetic acid / 1 h / 20 °C
2: 92 percent / aq. NaOH / methanol; diethyl ether / 1 h / 20 °C
View Scheme
参考文献
Korotkikh, N. I.; Aslanov, A. F.; Shvaika, O. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 6 p. 716 - 717
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 6 p. 855 - 856
反应条件
sodium hydroxide; tetrabutylammomium bromide
T=45 - 55°C; Rearrangement; disproportionation; 25 h; Further byproducts given;
参考文献
Ramazanova; Tarakanova; Vagabov; Litvinova; Anisimov
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 2 p. 201 - 206
