N,N-二乙基-3-苯基-2-丙炔-1-胺合成路线 （共 21 条）
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; copper(l) chloride in acetonitrile
T=60°C; 14 h; Inert atmosphere;
参考文献
Yu, Dingyi; Zhang, Yugen
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 163 - 169
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; copper(l) chloride in acetonitrile
T=60°C; 14 h; Inert atmosphere;
参考文献
AGENCY FOR SCIENCE, TECHNOLOGY AND RESEARCH; ZHANG, Yugen; YU, Dingyi
Patent: WO2012/5692 A1, 2012 ;
Location in patent: Page/Page column 10; 12 ;
反应条件
copper(l) iodide; potassium carbonate; Tedicyp; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide
T=110°C; 20 h;
参考文献
Lemhadri, Mhamed; Doucet, Henri; Santelli, Maurice
Synthesis, 2005 , # 8 art. no. Z22104SS, p. 1359 - 1367
反应条件
copper dichloride
T=80°C; Mannich reaction; P=150.015 Torr; 3 h;
参考文献
Sharifi, Ali; Mirzaei, Mojtaba; Naimi-Jamal, M. Reza
Journal of Chemical Research, 2007 , # 2 p. 129 - 132
反应条件
copper(l) iodide; potassium carbonate; Tedicyp; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide
T=110°C; 20 h;
参考文献
Lemhadri, Mhamed; Doucet, Henri; Santelli, Maurice
Synthesis, 2005 , # 8 art. no. Z22104SS, p. 1359 - 1367
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; copper(l) chloride in acetonitrile
T=60°C; 14 h; Inert atmosphere;
参考文献
Yu, Dingyi; Zhang, Yugen
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 163 - 169
反应条件
silver(I) acetate in 1,4-dioxane
T=120°C; 6 h;
参考文献
Chen, Xiuling; Chen, Tieqiao; Zhou, Yongbo; Au, Chak-Tong; Han, Li-Biao; Yin, Shuang-Feng
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 2 p. 247 - 250
反应条件
silver(I) acetate in 1,4-dioxane
T=120°C; 12 h; Inert atmosphereSchlenk techniqueSealed tube; Reagent/catalystSolvent;
参考文献
Chen, Xiuling; Chen, Tieqiao; Zhou, Yongbo; Au, Chak-Tong; Han, Li-Biao; Yin, Shuang-Feng
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 2 p. 247 - 250
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; silver fluoride; sodium hydrogencarbonate in acetonitrile
T=20°C; 3 h;
参考文献
Ye, Zhishi; Liu, Miaochang; Lin, Baoda; Wu, Huayue; Ding, Jinchang; Cheng, Jiang
Tetrahedron Letters, 2009 , vol. 50, # 5 p. 530 - 532
反应条件
N-chloro-succinimide; CuCl2·2H2O; sodium hydrogencarbonate in toluene
T=20 - 110°C; 6 h; Inert atmosphere;
参考文献
Zhu, Yefeng; Zhao, Huishuang; Wei, Yunyang
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-H0052-OP, p. 952 - 958
