1,11-二氰基-3,6,9-氧杂-十一烷合成路线 （共 16 条）
反应条件
sodium hydroxide in water T=0 - 20°C;
参考文献
Zhang, Yong; Fu, Qi; Shi, Wenfang
Science China Chemistry, 2010 , vol. 53, # 12 p. 2452 - 2460
反应条件
sodium hydroxide 1) benzene, 70 to 80 deg C.; Yield given. Multistep reaction;
参考文献
Movsumzade, E. M.; Rasulbekova, T. I.; Kulieva, D. A.; Aliev, G. R.; Movsumzade, S. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 11 p. 2132 - 2135
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 11 p. 2334 - 2337
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 3; 4 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in tert-butyl methyl ether T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4-5; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in methanol T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt T=125°C; P=47304.6 Torr; 4 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4-5; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in water T=60°C; P=42133 Torr; 4 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 3; 6 ;
反应条件
hydrogen; nickel in ethanol
参考文献
Chekulaeva,I.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 1752 - 1754
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1829 - 1832
反应条件
hydrogen; Grace 2724 sponge cobalt in tert-butyl methyl ether T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4-5; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in methanol T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4; 7 ;
