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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
224-11-3
合成路线
（共 46 条）
109512-11-0
→
反应条件
224-11-3
反应条件
hydrogen; palladium on activated charcoal in methanol T=18°C; P=760 Torr; 10 h;
参考文献
Banwell, Martin G.; Lupton, David W.; Ma, Xinghua; Renner, Jens; Sydnes, Magne O.
Organic Letters, 2004 , vol. 6, # 16 p. 2741 - 2744
161196-33-4
→
反应条件
224-11-3
反应条件
potassium hydroxide; hydrogen; palladium on activated charcoal in methanol; toluene T=18°C; P=760 Torr; 24 h;
参考文献
Banwell, Martin G.; Cowden, Cameron J.
Australian Journal of Chemistry, 1994 , vol. 47, # 12 p. 2235 - 2254
67342-71-6
→
反应条件
224-11-3
反应条件
1,10-phenanthroline; potassium tert-butylate in 1,3,5-trimethyl-benzene T=110°C; 8 h; Inert atmosphereSchlenk techniqueSealed tube; Reagent/catalystTime;
参考文献
De, Subhadip; Mishra, Sourabh; Kakde, Badrinath N.; Dey, Dhananjay; Bisai, Alakesh
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 7823 - 7844
115377-94-1
2-BOC-氨基苯基硼酸
+
15930-53-7
6-溴-3,4-亚甲基二氧苯甲醛
→
反应条件
224-11-3
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether Suzuki Coupling; Inert atmosphere;
参考文献
Baechler, Simone A.; Fehr, Markus; Habermeyer, Michael; Hofmann, Andreas; Merz, Karl-Heinz; Fiebig, Heinz-Herbert; Marko, Doris; Eisenbrand, Gerhard
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 3 p. 814 - 823
1039078-51-7
→
反应条件
224-11-3
反应条件
1-ethyl-3-methyl-1H-imidazol-3-ium hexafluorophosphate in toluene T=160°C; 0.5 h; microwave irradiation;
参考文献
Portela-Cubillo, Fernando; Scott, Jackie S.; Walton, John C.
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5558 - 5565
880643-56-1
→
反应条件
224-11-3
反应条件
fumaric acid diethyl ester; palladium on activated charcoal in diphenylether 5 h; Heating;
参考文献
Kumemura, Teppei; Choshi, Tominari; Yukawa, Junko; Hirose, Aya; Nobuhiro, Junko; Hibino, Satoshi
Heterocycles, 2005 , vol. 66, # 1 p. 87 - 90
141-32-2
丙烯酸丁酯
+
1360593-35-6
→
反应条件
224-11-3
反应条件
oxygen; copper diacetate; palladium dichloride in N,N-dimethyl acetamide T=140°C; P=760.051 Torr; 48 h;
参考文献
Liu, Yan-Yun; Song, Ren-Jie; Wu, Cui-Yan; Gong, Lu-Bin; Hu, Ming; Wang, Zhi-Qiang; Xie, Ye-Xiang; Li, Jin-Heng
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 347 - 353
15930-53-7
6-溴-3,4-亚甲基二氧苯甲醛
→
反应条件
224-11-3
反应条件
1: 99 percent / NaOMe / PdCl2(PPh3)2 / methanol / 0.08 h / microwave irradiation 2: 97 percent / AcONa / ethanol / 1 h / 80 °C 3: 90 percent / various solvent(s) / 1 h / 180 °C / microwave irradiation 4: 86 percent / diethyl fumarate / Pd/C / diphenyl ether / 5 h / Heating View Scheme
参考文献
Kumemura, Teppei; Choshi, Tominari; Yukawa, Junko; Hirose, Aya; Nobuhiro, Junko; Hibino, Satoshi
Heterocycles, 2005 , vol. 66, # 1 p. 87 - 90
1449388-51-5
→
反应条件
224-11-3
反应条件
1,10-phenanthroline; potassium tert-butylate in 1,3,5-trimethyl-benzene T=110°C; 20 h; Inert atmosphereSchlenk techniqueSealed tube; Reagent/catalystTime;
参考文献
De, Subhadip; Mishra, Sourabh; Kakde, Badrinath N.; Dey, Dhananjay; Bisai, Alakesh
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 7823 - 7844
1449388-52-6
→
反应条件
224-11-3
反应条件
1,10-phenanthroline; potassium tert-butylate in 1,3,5-trimethyl-benzene T=110°C; 20 h; Inert atmosphereSchlenk techniqueSealed tube; Reagent/catalystTime;
参考文献
De, Subhadip; Mishra, Sourabh; Kakde, Badrinath N.; Dey, Dhananjay; Bisai, Alakesh
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 7823 - 7844
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