反应条件
1: (COCl)2; DMF / tetrahydrofuran / 2.5 h / Heating
2: 3.53 g / Et3N / tetrahydrofuran / 3 h / 20 °C
3: 84 percent / NaH / dimethylformamide / 1.5 h / 20 °C
4: Ag2CO3; PPh3 / Pd(OAc)2 / dimethylformamide / 2 h / Heating
5: LAH / tetrahydrofuran / 3 h / 20 °C
6: 38 mg / aq. HCl / 1 h / 80 °C
View Scheme
参考文献
Harayama, Takashi; Akamatsu, Hisashi; Okamura, Kana; Miyagoe, Taeko; Akiyama, Toshihiko; Abe, Hitoshi; Takeuchi, Yasuo
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 5 p. 523 - 528
