3,3,3-三氟-1-丙醇合成路线 （共 15 条）
反应条件
1: With borane-THF T=20°C; Hydroboration; 2: With dihydrogen peroxide Oxidation;
参考文献
Angewandte Chemie - International Edition, , vol. 38, # 13-14 p. 2052 - 2054
反应条件
tetrakis(dimethylamino)ethylene in tetrahydrofuran T=-20 - 20°C;
参考文献
Organic Letters, , vol. 4, # 26 p. 4671 - 4672
反应条件
1: With [Rh(COD)(dppb)](1+)*BF4(1-) in tetrahydrofuran T=-25°C; 0.75 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran Further stages. Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 1, # 9 p. 1399 - 1402
反应条件
1: With Wilkinson's catalyst in tetrahydrofuran T=20°C; 2 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran Further stages. Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 1, # 9 p. 1399 - 1402
反应条件
potassium hydroxide; benzyl-tri-(n-butyl)-ammonium bromide T=75 - 80°C; 0.333333 h;
参考文献
Golding,B.T.; Sellars,P.J.
Journal of Fluorine Chemistry, 1985 , vol. 30, p. 153
反应条件
diethyl ether; oxygen; magnesium
参考文献
Journal of the American Chemical Society, , vol. 70, p. 2911
参考文献
Journal of the Chemical Society, , p. 1273,1278
反应条件
oxygen Pulsed laser photolysisGas phase; Quantum yield; Pressure;
参考文献
Journal of Photochemistry and Photobiology A: Chemistry, , vol. 231, # 1 p. 33 - 40
反应条件
sodium carbonate in tetrahydrofuran
参考文献
Hierse, Wolfgang; Ignatyev, Nikolai (Mykola); Seidel, Martin; Montenegro, Elvira; Kirsch, Peer; Bathe, Andreas
Patent: US2010/152081 A1, 2010 ;
反应条件
sodium dichromate; sulfuric acid T=85 - 90°C; 0.333333 h;
参考文献
Golding,B.T.; Sellars,P.J.
Journal of Fluorine Chemistry, 1985 , vol. 30, p. 153
