3-氯-4’-甲基苯丙酮合成路线 （共 15 条）
反应条件
aluminium trichloride; nitromethane in carbon disulfide 2 h; Ambient temperature;
参考文献
Khalaf, Ali A.; Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; El-Zohry, Maher F.
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 7-8 p. 285 - 291
反应条件
AlCl3, aluminium chloride in carbon disulfide T=20°C; 0.25 h; Inert atmosphere;
参考文献
Bertolini, Ferruccio; Crotti, Stefano; Di Bussolo, Valeria; Macchia, Franco; Pineschi, Mauro
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8998 - 9007
参考文献
Khalaf, Ali A.; Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; El-Zohry, Maher F.
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 7-8 p. 285 - 291
反应条件
boron trifluoride diethyl etherate; Petroleum ether
参考文献
Izvestiya Vysshikh Uchebnykh Zavedenii, Khimiya i Khimicheskaya Tekhnologiya, , vol. 2, p. 895
Chem.Abstr., , p. 12046
反应条件
potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane T=80°C; 20 h; Inert atmosphere;
参考文献
Jiang, Quanbin; Guo, Tenglong; Wang, Qingfu; Wu, Ping; Yu, Zhengkun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1874 - 1880
反应条件
potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane T=80°C; 20 h; Inert atmosphere; Overall yield = 57 percent; Overall yield = 136 mg;
参考文献
Jiang, Quanbin; Guo, Tenglong; Wang, Qingfu; Wu, Ping; Yu, Zhengkun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1874 - 1880
反应条件
sulfuric acid in neat (no solvent) T=90°C; 1 h;
参考文献
Khalaf, Ali A.; Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; El-Zohry, Maher F.
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 7-8 p. 285 - 291
反应条件
sulfuric acid T=95°C; 2 h;
参考文献
Boberg, Friedrich; Deters, Karin; Schulz, Juergen; Torges, Karl-Franz
Phosphorus, Sulfur and Silicon and the Related Elements, 1994 , vol. 91, # 1-4 p. 69 - 80
反应条件
sulfuric acid in neat (no solvent) T=90°C; 1 h;
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 7-8 p. 285 - 291
反应条件
potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane T=80°C; 20 h; Inert atmosphere; Overall yield = 57 percent; Overall yield = 136 mg;
参考文献
Jiang, Quanbin; Guo, Tenglong; Wang, Qingfu; Wu, Ping; Yu, Zhengkun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1874 - 1880
