3-氯-1-(2,4-二甲基苯基)丙-1-酮合成路线 (共 4 条)
反应条件
aluminium trichloride in dichloromethane 2 h;
参考文献
Neudeck
Monatshefte fur Chemie, 1996 , vol. 127, # 2 p. 185 - 200
反应条件
1: H2SO4 2: LiAlH4 / diethyl ether 3: oxalic acid / H2O / Heating View Scheme
参考文献
Marechal,E. et al.
Bulletin de la Societe Chimique de France, 1969 , p. 1981 - 1989
反应条件
sulfuric acid T=100°C; 1 h;
参考文献
Neudeck
Monatshefte fur Chemie, 1996 , vol. 127, # 2 p. 185 - 200
反应条件
potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane
T=80°C; 20 h; Inert atmosphere;
参考文献
Jiang, Quanbin; Guo, Tenglong; Wang, Qingfu; Wu, Ping; Yu, Zhengkun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1874 - 1880