5-苄氧基-2-硝基甲苯合成路线 （共 18 条）
反应条件
hydrogen; nickel 1) DMF, 140 degC, 16 h.; 2) EtOH; Yield given. Multistep reaction;
参考文献
Taydakov; Dutova; Sidorenko; Krasnoselsky
Chemistry of Heterocyclic Compounds, 2011 , vol. 47, # 4 p. 425 - 434
反应条件
1: 91 percent / 14 h / 110 °C 2: 1.) hydrazine monohydrate, nickel boride / 1.) ethanol, 80 deg C, 0.5 h, 2.) ethanol, 50 deg C, 3 h View Scheme
参考文献
Taydakov; Dutova; Sidorenko; Krasnoselsky
Chemistry of Heterocyclic Compounds, 2011 , vol. 47, # 4 p. 425 - 434
反应条件
hydrazine hydrate; nickel 1.) reflux, 3 h, 2.) THF, MeOH, RT, 30 min; Multistep reaction;
参考文献
Buchheit; Gamse; Giger; Hoyer; Klein; Kloeppner; Pfannkuche; Mattes
Journal of medicinal chemistry, 1995 , vol. 38, # 13 p. 2331 - 2338
反应条件
1: potassium ethylate; diethyl ether 2: FeSO4; aqueous NaOH View Scheme
参考文献
Journal of the Chemical Society, , p. 49
参考文献
Ohkubo, Mitsuru; Nishimura, Teruyuki; Jona, Hideki; Honma, Teruki; Morishima, Hajime
Tetrahedron, 1996 , vol. 52, # 24 p. 8099 - 8112
反应条件
1: potassium ethylate; diethyl ether 2: FeSO4; aqueous NaOH 3: palladium/charcoal; methanol / Hydrogenation View Scheme
参考文献
Bergel; Morrison
Journal of the Chemical Society, 1943 , p. 49
反应条件
1: in N,N-dimethyl-formamide
24 h; Heating;
2: With hydrogenchloride in diethyl ether
2 h; Heating; Further stages.;
参考文献
Li, Xin; Abell, Chris; Congreve, Miles S.; Warrington, Brian H.; Ladlow, Mark
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 7 p. 989 - 998
反应条件
1: potassium ethylate; diethyl ether
2: FeSO4; aqueous NaOH
3: HCl
4: palladium/charcoal; methanol / Hydrogenation
View Scheme
参考文献
Bergel; Morrison
Journal of the Chemical Society, 1943 , p. 49
