4-羟基环己酮乙二醇缩醛合成路线 （共 42 条）
反应条件
sodium tetrahydroborate in methanol 2.5 h;
参考文献
CRYPTOPHARMA PTY LTD
Patent: WO2008/124878 A1, 2008 ;
Location in patent: Page/Page column 82-83 ;
反应条件
toluene-4-sulfonic acid in ethylene glycol; benzene
反应条件
hydrogenchloride in methanol; 1-t-Butyl carbamate-3-trifluoromethane sulfonoxy-1-cyclopentane-1-carboxylic carboxylic acid methyl ester
反应条件
sodium hydroxide; sodium borohydride in methanol
反应条件
sodium borohydride in diethyl ether; ethanol
反应条件
triethylsilane; NaPF6; dirhenium heptaoxide in dichloromethane T=50°C; 60 h; chemoselective reaction;
参考文献
Das, Braja Gopal; Ghorai, Prasanta
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 26 p. 4379 - 4382
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Hwu; Leopold
Journal of the Chemical Society - Series Chemical Communications, 1984 , vol. NO. 11, p. 721 - 723
反应条件
toluene-4-sulfonic acid; benzene Erwaermen des Reaktionsprodukts mit methanol. Natronlauge;
参考文献
Helvetica Chimica Acta, , vol. 40, p. 1621,1625
反应条件
1: 4.84 g / conc. H2SO4 / benzene / Heating 2: 98 percent / NaBH4 / methanol / 1.) 0 deg C, 0.5 h, 2.) room temperature, 1 h View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 6 p. 1221 - 1234
反应条件
toluene-4-sulfonic acid; benzene
参考文献
Chemische Berichte, , vol. 90, p. 1973,1944
