2,3,4,5,6-五甲基苯甲酸合成路线 (共 17 条)
参考文献
Smith; Webster; Guss
Journal of the American Chemical Society, 1937 , vol. 59, p. 1078,1080
反应条件
palladium diacetate in acetic acid
7 h; Heating; Yield given;
参考文献
Itahara, Toshio; Kawasaki, Kazukuni; Ouseto, Fumio
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 11 p. 3488 - 3493
反应条件
aluminium trichloride
T=-10°C;
参考文献
Jacobsen
Chemische Berichte, 1889 , vol. 22, p. 1217
反应条件
3,3-dimethyldioxirane in acetone
24 h; Ambient temperatureother reaction time, temperature, effect of amount of oxidant. effect of additives; Product distribution;
参考文献
Murray, Robert W.; Singh, Megh; Rath, Nigam
Journal of Organic Chemistry, 1997 , vol. 62, # 25 p. 8794 - 8799
反应条件
nitric acid; acetic anhydride; sodium carbonate
1.) 0 deg C, 2 h, 2.) 0 deg C to RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Keumi, Takashi; Morita, Toshio; Teramoto, Koichi; Takahashi, Hisakazu; Yamamoto, Hiroshi; et al.
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3439 - 3446
参考文献
Jacobsen
Chemische Berichte, 1889 , vol. 22, p. 1217
反应条件
Pb(II) thiocyanate
T=200 - 230°C;
参考文献
Rudenko; Salfetnikova; Vasil'ev
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 10 p. 1447 - 1470