反应条件
1: pyridine / 24 h / 50 °C
2: pyridine / 24 h / 20 °C
3: 98 percent / aq. CF3COOH / 0.08 h
4: 89 percent / pyridine / 24 h / 20 °C
5: 93 percent / MeONa / dimethylformamide / 0.25 h / 40 °C / 20 Torr
6: 97 percent / NaOMe / methanol / 4 h / 20 °C
7: Cl2 / CH2Cl2 / 0.25 h / 0 °C
8: 58 percent / NaCNBH3 / acetic acid / 24 h / 20 °C
View Scheme
参考文献
Fuentes, Jose; Gasch, Consolacion; Olano, David; Pradera; Repetto, Guillermo; Sayago, Francisco J.
Tetrahedron Asymmetry, 2002 , vol. 13, # 16 p. 1743 - 1753
