zinc(II) chloride

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<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11342940', constants.ctx, '0')">sodium hydroxide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '19402851', constants.ctx, '0')">C₁₂H₂₂S</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3916152', constants.ctx, '0')">tetra-(n-butyl)ammonium iodide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=20 - 25&deg;C;&nbsp;40&nbsp;h;&nbsp;&nbsp;optical yield given as percent eeenantioselective reaction;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 96 percent / methanol / 0.5 h<br />2: NaOMe / methanol<br />3: chiral deriv. of [2-thiabicyclohept-3-yl]bicycloheptanone; benzyltriethylammonium chloride; rhodium(II) acetate dimer / acetonitrile / 48 h / 40 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1.1: dioxane / 0.5 h / 20 &deg;C<br />1.2: NaH / 1 h / 20 &deg;C<br />2.1: C₁₅H₂₂OS; Rh₂(OAc)4; BnEt₃N⁽¹⁺⁾*Cl^(1-) / acetonitrile / 40 &deg;C<br /> <br /> &nbsp;