1,3-二甲基-5-碘苯合成路线 （共 74 条）
反应条件
4,4'-bis(trimethylaminomethyl)-2,2'-bipyridine dihydrobromide; bis-triphenylphosphine-palladium(II) chloride; water; sodium carbonate in water T=100°C; P=7600.51 Torr; 24 h; Autoclave; Catalytic behavior;
参考文献
Tsai, Sheng-Wen; Huang, Shao-Hsien; Lee, Han-Sheng; Tsai, Fu-Yu
Journal of the Chinese Chemical Society, 2013 , vol. 60, # 7 p. 769 - 772
反应条件
[Cu8(H){S2P(OiPr)2}6](PF6); caesium carbonate in N,N-dimethyl-formamide T=120°C; Ullmann-Goldberg type coupling; 24 h;
参考文献
Wu, Cheng-Chieh; Lee, Bo-Han; Liao, Ping-Kuei; Fang, Ching-Shiang; Liu
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 4 p. 480 - 484
反应条件
in benzene-d6 T=120°C;
参考文献
Delp, Samuel A.; Goj, Laurel A.; Pouy, Mark J.; Munro-Leighton, Colleen; Lee, John P.; Gunnoe, T. Brent; Cundari, Thomas R.; Petersen, Jeffrey L.
Organometallics, 2011 , vol. 30, # 1 p. 55 - 57
反应条件
(CuOTf)2.C6H6; caesium carbonate; 1,10-phenanthroline; (dibenzylidene)acetone in xylene T=110°C; Substitution; 30 h;
参考文献
Kiyomori, Ayumu; Marcoux, Jean-Francois; Buchwald, Stephen L.
Tetrahedron Letters, 1999 , vol. 40, # 14 p. 2657 - 2660
反应条件
hydrogen; potassium carbonate in 1,4-dioxane T=120 - 140°C; P=30003 Torr; 20 h; Autoclave;
参考文献
Applied Catalysis A: General, , vol. 469, p. 146 - 152
反应条件
copper(l) iodide; potassium carbonate; trans-N,N'-dimethylcyclohexane-1,2-diamine in n-butyronitrile T=70°C; 24 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, # 47 p. 17423 - 17429
反应条件
potassium phosphate; Pd0(tris(tert-butyl)phosphine)2 in 1-methyl-pyrrolidin-2-one T=20°C; 60 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 23 p. 9607 - 9609
反应条件
0.5C4H8O*C24H20B(1-)*C36H64CoN8(1+) in tetrahydrofuran T=-116 - 20°C; 6 h; Inert atmosphere;
参考文献
Mo, Zhenbo; Li, Yuxue; Lee, Hung Kay; Deng, Liang
Organometallics, 2011 , vol. 30, # 17 p. 4687 - 4694
反应条件
(2,5-diisopropyl-3,4-dimethyl-2,5-imidazol-1-ylidene)2Fe(NH-2,4,6-trimethylphenyl)2 T=50°C; 8 h; Inert atmosphere;
参考文献
Inorganic Chemistry, , vol. 52, # 1 p. 59 - 65
参考文献
Klages; Liecke
Journal fuer Praktische Chemie (Leipzig), 1900 , vol. <2> 61, p. 322
