1,3-二甲基-5-碘苯合成路线 （共 74 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; toluene Suzuki coupling; 3 h; Heating;
参考文献
Choi; Hamilton
Journal of the American Chemical Society, 2001 , vol. 123, # 10 p. 2456 - 2457
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate T=110°C; 23 h;
参考文献
Wolter, Martina; Nordmann, Gero; Job, Gabriel E; Buchwald, Stephen L
Organic letters, 2002 , vol. 4, # 6 p. 973 - 976
反应条件
copper(l) iodide; 8-hydroxy-quinoline; potassium hydroxide in water; dimethyl sulfoxide; tert-butyl alcohol T=100°C; 48 h; Inert atmosphere;
参考文献
Synlett, , # 6 p. 976 - 978
反应条件
copper(l) iodide; TBANO2; N-methyl-2-(methylamino)ethylamine in 1-methyl-pyrrolidin-2-one T=100°C; 0.166667 h; Microwave irradiationInert atmosphere;
参考文献
Bulletin of the Korean Chemical Society, , vol. 33, # 2 p. 689 - 691
反应条件
copper(l) iodide; CsOH; 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate in dimethyl sulfoxide T=130°C; 30 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Tlili, Anis; Monnier, Florian; Taillefer, Marc
Chemistry - A European Journal, 2010 , vol. 16, # 41 p. 12299 - 12302
反应条件
potassium phosphate; copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; water in ethanol T=130°C; 30 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Tlili, Anis; Monnier, Florian; Taillefer, Marc
Chemistry - A European Journal, 2010 , vol. 16, # 41 p. 12299 - 12302
反应条件
Ag2CO3; palladium diacetate; potassium carbonate; acetic acid T=120°C; 24 h; Inert atmosphere;
参考文献
Arroniz, Carlos; Ironmonger, Alan; Rassias, Gerry; Larrosa, Igor
Organic Letters, 2013 , vol. 15, # 4 p. 910 - 913
反应条件
Ag2CO3; palladium diacetate; potassium carbonate; acetic acid T=120°C; 24 h; Inert atmosphere;
参考文献
Arroniz, Carlos; Ironmonger, Alan; Rassias, Gerry; Larrosa, Igor
Organic Letters, 2013 , vol. 15, # 4 p. 910 - 913
反应条件
N-methyl-2-(methylamino)ethylamine; copper(l) iodide in toluene T=110°C; 24 h;
参考文献
MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Patent: WO2004/13094 A2, 2004 ;
Location in patent: Page 61 ;
反应条件
triethylamine; nanostructured pyridine-functionalized silica Pd(II) complex in N,N-dimethyl-formamide 24 h; Heating;
参考文献
Polshettiwar, Vivek; Hesemann, Peter; Moreau, Joel J.E.
Tetrahedron, 2007 , vol. 63, # 29 p. 6784 - 6790
