1,3-二甲基-5-碘苯合成路线 （共 74 条）
反应条件
[NiCl2(1,2-dimethoxyethane)]; 1,3-bis-(diphenylphosphino)propane; water; zinc in ethylene glycol dimethyl ether
T=100°C; 36 h;
参考文献
Hsieh, Jen-Chieh; Chen, Yen-Chung; Cheng, An-Yi; Tseng, Hsiao-Chun
Organic Letters, 2012 , vol. 14, # 5 p. 1282 - 1285
反应条件
potassium permanganate in water; tert-butyl alcohol
T=100°C; 21 h;
参考文献
Wessendorf, Florian; Hirsch, Andreas
Tetrahedron, 2008 , vol. 64, # 50 p. 11480 - 11489
反应条件
1: 98 percent / triethylamine; bis(triphenylphosphine)palladium dichloride; copper(I) iodide / 4 h / 20 °C
2: 80 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.5 h / -15 °C
View Scheme
参考文献
Marchand, Pascal; Puget, Alain; Le Baut, Guillaume; Emig, Peter; Czech, Michael; Guenther, Eckhard
Tetrahedron, 2005 , vol. 61, # 16 p. 4035 - 4041
反应条件
trifuran-2-yl-phosphane; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium (0) in acetonitrile
T=40°C; 10 h;
参考文献
Arcadi; Cacchi; Cascia; Fabrizi; Marinelli
Organic letters, 2001 , vol. 3, # 16 p. 2501 - 2504
