Alpha,Alpha-二氟苯乙酸乙酯合成路线 （共 22 条）
反应条件
copper in dimethyl sulfoxide; N,N-dimethyl-formamide T=20°C; 12 h;
参考文献
Qi, Qingqing; Shen, Qilong; Lu, Long
Journal of the American Chemical Society, 2012 , vol. 134, # 15 p. 6548 - 6551
反应条件
triethylamine tris(hydrogen fluoride) in acetonitrile Ambient temperatureconstant potential electrolysis (Pt-electrode, E= 1,6 V);
参考文献
Brigaud, Thierry; Laurent, Andre; Laurent, Eliane
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 59, # 1-4 p. 153 - 156
反应条件
1.1: tetrahydrofuran / 0.5 h / 0 - 20 °C / |Inert atmosphere 2.1: trans-N,N,N′,N'-tetramethylcyclohexane-1,2-diamine; cobalt(II) chloride / tetrahydrofuran / 0.08 h / 20 °C / |Inert atmosphere 2.2: 22 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Tetrahedron, , vol. 69, # 19 p. 3913 - 3918
反应条件
platinum; Et3N-4HF T=25°C; Electrolysis;
参考文献
Journal of Fluorine Chemistry, , vol. 129, # 3 p. 185 - 192
反应条件
1: SbF3 2: concentrated H2SO4 3: aqueous NaOH 4: SOCl2 View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 772,774; engl. Ausg. S. 750, 752
反应条件
1: concentrated H2SO4 2: aqueous NaOH 3: SOCl2 View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 772,774; engl. Ausg. S. 750, 752
反应条件
1: SOCl2 View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 772,774; engl. Ausg. S. 750, 752
反应条件
1: aqueous NaOH 2: SOCl2 View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 772,774; engl. Ausg. S. 750, 752
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 772,774; engl. Ausg. S. 750, 752
反应条件
sodium hydroxide T=25°C;
参考文献
Middleton, W. J.; Bingham, E. M.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2883 - 2887
