Klumpp, Douglas A; Sanchez Jr., Gregorio V; Aguirre, Sharon L; Zhang, Yun; de Leon, Sarah
The Journal of organic chemistry, 2002 , vol. 67, # 14 p. 5028 - 5031
1: in toluene T=20°C; 2: With sulfuric acid; phosphorus pentoxide in toluene T=160°C; 1 h; 3: With sodium hydroxide in water; toluene pH=8; Cooling with ice;
1: para-bromobenzonitrile With sodium methylate in methanol T=20°C; 5.5 h; 2: 2-aminoacetaldehyde dimethyl acetal With acetic acid in methanol T=50°C; 1 h; 3: With hydrogenchloride in methanol T=65°C; 18 h;
Walker, Matthew D.; Andrews, Benjamin I.; Burton, Andrew J.; Humphreys, Luke D.; Kelly, Gary; Schilling, Mark B.; Scott, Peter W.
Organic Process Research and Development, 2010 , vol. 14, # 1 p. 108 - 113