14-硫氧代-二螺[5.1.5.1]-7-十四酮合成路线 (共 5 条)
反应条件
tetraphosphorus decasulfide in pyridine 2 h; Heating;
参考文献
Sundari, B.; Ramamurthy, V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 498 - 501
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Muthuramu, K.; Sundari, B.; Ramamurthy, V.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4482 - 4487
反应条件
hydrogenchloride; hydrogen sulfide; zinc(II) chloride in methanol; ethanol
参考文献
Journal of Organic Chemistry, , vol. 52, # 11 p. 2154 - 2161
反应条件
T=-70°C; 50 h; Irradiation;
参考文献
Kimura, Koji; Fukuda, Yoshihiro; Negoro, Toshihiko; Odaira, Yoshinobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 6 p. 1901 - 1902
反应条件
tetraphosphorus decasulfide in pyridine 2 h; Heating;
参考文献
Muthuramu, K.; Sundari, B.; Ramamurthy, V.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4482 - 4487
反应条件
triphenyl phosphite; ozone
1.) -80 deg C, methylene chloride 2.) room temperature, 2 h; Yield given. Multistep reaction;
参考文献
Sundari, B.; Ramamurthy, V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 498 - 501