N-乙氧羰基邻苯二甲酰亚胺合成路线 (共 86 条)
反应条件
in tetrahydrofuran 48 h; Heating;
参考文献
Chu, Lin; Fisher, Michael H.; Goulet, Mark T.; Wyvratt, Matthew J.
Tetrahedron Letters, 1997 , vol. 38, # 22 p. 3871 - 3874
反应条件
1: sodium carbonate / water / 1 h / 20 °C 2: 2,4,6-triphenylpyrylium-tetrafluoroborate / acetonitrile / 96 h / Inert atmosphere; Irradiation View Scheme
参考文献
Griesbeck, Axel G.; Neudoerfl, Joerg; Kiff, Alan De
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 518 - 524
反应条件
1: 86 percent / aq. K2CO3 / 0.5 h / Ambient temperature 2: 95 percent / PCC, molecular sieves 4A / CH2Cl2 / 3 h View Scheme
参考文献
AC Immune, S.A.
Patent: US2011/280808 A1, 2011 ;
反应条件
hydroxylamine hydrochloride; sodium methylate
参考文献
Neunhoeffer,O. et al.
Justus Liebigs Annalen der Chemie, 1968 , vol. 712, p. 208 - 213
反应条件
tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate in dichloromethane
参考文献
Dankwardt, Sharon M.; Ferla, Steven; Krstenansky, John L.; Bhakta, Sunil; Ostrelich, Helene; Jarnagin, Kurt
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 14 p. 1921 - 1926
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate research, , vol. 162, # 2 p. 227 - 235
反应条件
1: 95 percent / Et3N / tetrahydrofuran / 6 h / Ambient temperature 2: 1 N aq. HCl / acetone / 2 h / Heating View Scheme
参考文献
Teshima, Tadashi; Matsumoto, Takahiro; Wakamiya, Tateaki; Shiba, Tetsuo; Aramaki, Yoshio; Nakajima, Terumi; Kawai, Nobufumi
Tetrahedron, 1991 , vol. 47, # 20-21 p. 3305 - 3312
反应条件
hydrogenchloride Yield given. Multistep reaction;
参考文献
Teshima, Tadashi; Wakamiya, Tateaki; Aramaki, Yoshio; Nakajima, Terumi; Kawai, Nobufumi; Shiba, Tetsuo
Tetrahedron Letters, 1987 , vol. 28, # 30 p. 3509 - 3510
反应条件
1: [14C]-L-Tryptophan With sodium carbonate in water 2: N-ethoxycarbonylphthalimide in water T=20°C; 2 h;
参考文献
Suksiriworapong, Jiraphong; Sripha, Kittisak; Junyaprasert, Varaporn Buraphacheep
Polymer, 2010 , vol. 51, # 11 p. 2286 - 2295
反应条件
sodium carbonate in water
参考文献
Celgene Corporation
Patent: US5698579 A1, 1997 ;