N-乙氧羰基邻苯二甲酰亚胺合成路线 （共 86 条）
反应条件
1: 80 percent / tetrahydrofuran / 12 h / Ambient temperature
2: 80 percent / CrO3, 35percent H2SO4 / acetone / 3 h / Ambient temperature
View Scheme
参考文献
Korosec; Poljsak; Urleb
Archiv der Pharmazie, 1992 , vol. 325, # 4 p. 251 - 252
反应条件
in tetrahydrofuran
Ambient temperature;
参考文献
McArthur, Colin R.; Worster, Paul M.; Jiang, Ji-Long; Leznoff, Clifford
Canadian Journal of Chemistry, 1982 , vol. 60, p. 1836 - 1841
反应条件
pyridine
1.) reflux, 2.5 h, 2.) RT, 16 h;
参考文献
Neidlein, Richard; Greulich, Peter; Kramer, Walter
Helvetica Chimica Acta, 1993 , vol. 76, # 6 p. 2407 - 2417
反应条件
1: water / 3 h / 20 °C
2: potassium hydroxide / water; diethyl ether
View Scheme
参考文献
Zhang, Qi; Chen, Kai; Rao, Weihao; Zhang, Yuejun; Chen, Fa-Jie; Shi, Bing-Feng
Angewandte Chemie - International Edition, 2013 , vol. 52, # 51 p. 13588 - 13592
Angew. Chem., 2013 , vol. 125, # 51 p. 13833 - 13837,5
反应条件
sodium carbonate in tetrahydrofuran
24 h; Ambient temperature; Yield given;
参考文献
Grote, Christopher W.; Kim, Dong Jin; Rapoport, Henry
Journal of Organic Chemistry, 1995 , vol. 60, # 21 p. 6987 - 6997
反应条件
sodium carbonate
T=20°C; 0.833333 h;
参考文献
Nakamura, Takanori; Noguchi, Tomomi; Miyachi, Hiroyuki; Hashimoto, Yuichi
Chemical and Pharmaceutical Bulletin, 2007 , vol. 55, # 4 p. 651 - 654
反应条件
potassium chloride in water; acetonitrile
T=30°C; ionic strength 1.0; various pH (MeNHOH as buffer; acetate buffer); N-methylhydroxylaminolysis of N-ethoxycarbonylphthalimide; general acid-base catalysis; Rate constant;
参考文献
Khan, M. Niyaz
International Journal of Chemical Kinetics, 1997 , vol. 29, # 9 p. 647 - 654
反应条件
in water; acetonitrile
T=30°C; pH=5.55; Kinetics; Further Variations:pH-values;
参考文献
Khan, N. Niyaz
International Journal of Chemical Kinetics, 2002 , vol. 34, # 2 p. 95 - 103
反应条件
1: 63 percent / Na2CO3 / H2O / 1 h / 25 °C
2: SOCl2 / dimethylformamide; CHCl3 / 2 h / Heating
3: Et3N / dimethylformamide; CH2Cl2 / 1.) -35 deg C, 30 min, 2.) 25 deg C, 3 h
4: 87 percent / BF3-etherate / tetrahydrofuran; ethyl acetate / 25 °C
5: 12 percent / acetone / 1 h / 10 - 20 °C / Irradiation
6: 53 percent / Raney Ni / ethanol / 2 h / Heating
View Scheme
参考文献
Wada, Masao; Nakai, Hideo; Sato, Yasuhiko; Hatanaka, Yasumaru; Kanaoka, Yuichi
Tetrahedron, 1983 , vol. 39, # 16 p. 2691 - 2698
反应条件
sodium carbonate in water
1 h; Ambient temperature;
参考文献
Gani, David; Young, Douglas W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2393 - 2398
