反应条件
copper(l) iodide in tetrahydrofuran
in sealed evacuated ampule; mixt. of Et3GeLi and CuI (equimol. amt.) inTHF stirred at -30°C for 30 min; pentafluorobenzoyl chloride added; stirred for 1 h while being gradually brought to room temp.; hexane added; ppt. filtered off; product isolated by fractionation of the yellow soln.; GLC; mass-spectrometry; NMR; elem. anal.;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Kalikhman, I. D.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 51 - 60
