2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride; magnesium iodide 1.) toluene, ether, -60 deg C, 2-5 h, 2.) 70 deg C, 1-2 h; Yield given. Multistep reaction. Yields of byproduct given;

2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride; magnesium iodide 1.) toluene, ether, -60 deg C, 2-5 h, 2.) 70 deg C, 1-2 h; Yield given. Multistep reaction. Yields of byproduct given;

<b>Multi-step reaction with 2 steps<br /> </b>1: hydrogen peroxide / 10 h / 5 &deg;C<br />2: 1.) 9-borabicyclo&lt;3.3.1&gt;nonane (9-BBN), 2.) monoethanolamine / 1.) THF, RT, overnight, 2.) diethyl ether<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11343078', constants.ctx, '0')">sodium tetrahydroborate</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '13283155', constants.ctx, '0')">Zn(ClO₄)2</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1696894', constants.ctx, '0')">diethyl ether</a> <br />&nbsp;1.) -78 deg C, 1 h; 2.) 0 deg C, 1 h;&nbsp;<br /> &nbsp;