1-(2,4-二硝基苯基)硫基-2,4-二硝基苯合成路线 （共 56 条）
反应条件
sodium azide; hexadecyltributylphosphonium thiocyanate in water; chlorobenzene
T=25°C; various temp.; Rate constant;
参考文献
Landini, Dario; Maia, Angelamaria; Montanari, Fernando
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 461 - 466
反应条件
1: 90 percent / (C16H33)Bu3P(1+)*SCN(1-) / chlorobenzene; H2O / 25 °C
2: tetrabutylammonium halide / chlorobenzene / 60 h
View Scheme
参考文献
Landini, Dario; Maia, Angelamaria; Montanari, Fernando
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 461 - 466
反应条件
potassium hydroxide; diethylene glycol monobutyl ether; potassium iodide
参考文献
Bost et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 1968
反应条件
1: 92 percent / LiH / dimethylsulfoxide / 3 h
2: Dinitro-fluoro-benzen, Triethylamin / tetrahydrofuran / Heating
View Scheme
参考文献
Augustin, Manfred; Guenther, Eckhard
Monatshefte fuer Chemie, 1990 , vol. 121, # 12 p. 1005 - 1015
反应条件
phenyl (2,2-dimethyl-4,6-dideoxo-1,3-dioxolan-5-yl)thiocarbamide; triethylamine in tetrahydrofuran
Heating;
参考文献
Augustin, Manfred; Guenther, Eckhard
Monatshefte fuer Chemie, 1990 , vol. 121, # 12 p. 1005 - 1015
反应条件
p-tolyl (2,2-dimethyl-4,6-dideoxo-1,3-dioxolan-5-yl)thiocarbamide; triethylamine in tetrahydrofuran
Heating;
参考文献
Augustin, Manfred; Guenther, Eckhard
Monatshefte fuer Chemie, 1990 , vol. 121, # 12 p. 1005 - 1015
反应条件
1-fluoro-2,4-dinitrobenzene; triethylamine in tetrahydrofuran
Heating;
参考文献
Augustin, Manfred; Guenther, Eckhard
Monatshefte fuer Chemie, 1990 , vol. 121, # 12 p. 1005 - 1015
反应条件
Fluorodinitrobenzene; triethylamine in tetrahydrofuran
Heating;
参考文献
Augustin, Manfred; Guenther, Eckhard
Monatshefte fuer Chemie, 1990 , vol. 121, # 12 p. 1005 - 1015
反应条件
hexadecyltributylphosphonium thiocyanate in water; chlorobenzene
T=25°C; various temp.; Rate constant;
参考文献
Landini, Dario; Maia, Angelamaria; Montanari, Fernando
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 461 - 466
反应条件
tetrabutylammonium halide in chlorobenzene
60 h;
参考文献
Landini, Dario; Maia, Angelamaria; Montanari, Fernando
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 461 - 466
