(3-甲基丁-2-烯基)丙二酸二乙酯合成路线 （共 59 条）
反应条件
sodium hydride; bis-diphenylphosphinoethane; Pd(1,2-bis(diphenylphosphino)ethane)2 in tetrahydrofuran
36 h; Heating;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
反应条件
1: 85 percent / NaOEt / ethanol / 1 h / Heating
2: 99 percent Spectr. / Et3Al / NiBr2(PPh3)2 / toluene / 24 h / 20 °C
View Scheme
参考文献
Necas, David; Tursky, Matyas; Kotora, Martin
Journal of the American Chemical Society, 2004 , vol. 126, # 33 p. 10222 - 10223
反应条件
1: 91 percent Spectr. / Et3Al; RuCl2(PPh3)3 / toluene / 36 h / 20 °C
2: 85 percent / NaOEt / ethanol / 1 h / Heating
3: 99 percent Spectr. / Et3Al / NiBr2(PPh3)2 / toluene / 24 h / 20 °C
View Scheme
参考文献
Necas, David; Tursky, Matyas; Kotora, Martin
Journal of the American Chemical Society, 2004 , vol. 126, # 33 p. 10222 - 10223
反应条件
1: 85 percent / NaOEt / ethanol / 1 h / Heating
2: 99 percent Spectr. / Et3Al / NiBr2(PPh3)2 / toluene / 24 h / 20 °C
View Scheme
参考文献
Necas, David; Tursky, Matyas; Kotora, Martin
Journal of the American Chemical Society, 2004 , vol. 126, # 33 p. 10222 - 10223
反应条件
sodium hydride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 36 h; Yield given. Yields of byproduct given;
参考文献
Alvarez, Eleuterio; Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1988 , vol. 339, p. 199 - 212
反应条件
NaCH(CO2Et)2; bis-diphenylphosphinoethane; bis(dibenzylideneacetone)-palladium(0) in dimethyl sulfoxide
T=100°C; 16 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Suzuki, Osamu; Hashiguchi, Yoshiharu; Inoue, Seiichi; Sato, Kikumasa
Chemistry Letters, 1988 , p. 291 - 294
反应条件
sodium hydride in tetrahydrofuran
Heating;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
反应条件
sodium hydride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 36 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Alvarez, Eleuterio; Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1988 , vol. 339, p. 199 - 212
反应条件
sodium hydride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 36 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Alvarez, Eleuterio; Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1988 , vol. 339, p. 199 - 212
反应条件
sodium hydride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 36 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Alvarez, Eleuterio; Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1988 , vol. 339, p. 199 - 212
