反应条件
1: 11.7 g / pyridine / H2O / 2 h / Heating
2: 18.4 g / lithium aluminium hydride / diethyl ether / 1.) 0 deg C, 2.) reflux, 1 h
3: 1.) toluene-p-sulphonyl chloride,pyridine, 2.) sodium iodide / 1.) 24 h, 2.) acetone, reflux, 16 h
View Scheme
参考文献
Cocker, Wesley; Geraghty, Niall W. A.; McMurry, T. Brian H.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2245 - 2254
