tetraphosphorus decasulfide; 1,2,3,4-tetrahydro-naphthalene

1: 79 percent / acetic acid / 1.) reflux, 10 h, 2.) r.t., overnight 2: 93 percent / 4 h / Heating 3: 69 percent / conc. aq. NH3 / ethanol / Ambient temperature 4: 75 percent / 2percent aq. HCl / 0.75 h / Heating 5: 55 percent / 4 h / Heating 6: 71 percent / conc. aq. NH3 / ethanol / 24 h / Ambient temperature 7: 63 percent / 2percent aq. HCl / ethanol / 50 h / Heating View Scheme

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1: P2S5; tetralin 3: diethyl ether 4: aqueous acetic acid 5: aq.-ethanolic HCl 6: aq.-ethanolic NaOH View Scheme

1: P2S5; tetralin 3: diethyl ether 4: aqueous acetic acid View Scheme

1: P2S5; tetralin 3: diethyl ether 4: aqueous acetic acid 6: aq.-ethanolic HCl View Scheme