2-甲氧基-4-[(e)-2-硝基乙烯基]苯酚合成路线 (共 19 条)
反应条件
ethylenediamine 3 h; Reflux;
参考文献
Yang, Jianxin; Dong, Jing; Lue, Xia; Zhang, Qiang; Ding, Wei; Shi, Xiaoxin
Chinese Journal of Chemistry, 2012 , vol. 30, # 12 p. 2827 - 2833
反应条件
methanol; amberlyst-15 in toluene T=110°C;
参考文献
Petchmanee, Thaninee; Ploypradith, Poonsakdi; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 7 p. 2892 - 2895
反应条件
ammonium cerium(IV) nitrate in acetonitrile T=20°C; 2 h;
参考文献
Sridhar Rao; Srinivas; Suresh Babu; Madhusudana Rao
Tetrahedron Letters, 2005 , vol. 46, # 47 p. 8141 - 8143
反应条件
iodine in 1,2-bis-(2-hydroxyethoxy)-ethane T=120°C; 3 h;
参考文献
Anuradha; Srinivas, Pullela V.; Ranga Rao; Manjulatha; Purohit, Muralidhar G.; Madhusudana Rao
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 20 p. 6820 - 6826
反应条件
cerium(IV) ammonium nitrate supported on silica; magnesium sulfate in dichloromethane T=20°C; 0.166667 h;
参考文献
Messere, Anna; Gentili, Alessandra; Garella, Isidoro; Temussi, Fabio; Di Blasio, Benedetto; Fiorentino, Antonio
Synthetic Communications, 2004 , vol. 34, # 18 p. 3317 - 3324
反应条件
ethanol Versetzen der roten Reaktionsloesung mit wss. HCl;
参考文献
Makarow
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2> 141, p. 77,89
Zhurnal Obshchei Khimii, 1935 , vol. 5, p. 39,47
反应条件
4-(N,N-dimethlyamino)pyridine; oxalyl dichloride; N,N-dimethyl-formamide 1) CHCl3, r.t., 3 h, 2) CHCl3, r.t., 72 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Peterli; Stumpf; Schweizer; Sequin; Mett; Traxler
Helvetica Chimica Acta, 1992 , vol. 75, # 3 p. 696 - 706
参考文献
Armarego,W.L.F.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 986 - 990
反应条件
1: NaBH4 2: H2 / Pd/C View Scheme
参考文献
Cederbaum, Fredrik; De Mesmaeker, Alain; Jeanguenat, Andre; Kempf, Hans-Joachim; Lamberth, Clemens; Schnyder, Anita; Zeller, Martin; Zeun, Ronald
Chimia, 2003 , vol. 57, # 11 p. 680 - 684
反应条件
T=25°C; Rate constant;
参考文献
Stewart
Journal of the American Chemical Society, 1952 , vol. 74, p. 4531,4533