2-苯基乙基异硫代氰酸酯合成路线 （共 33 条）
反应条件
1: phenethylamine With 1,4-diaza-bicyclo[2.2.2]octane; carbon disulfide T=20°C; 12 h; 2: bis(trichloromethyl) carbonate Reflux;
参考文献
Chemical Biology and Drug Design, , vol. 76, # 1 p. 25 - 33
反应条件
1: dioxane / Heating 2: 5 h / 150 - 200 °C View Scheme
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 314, # 5 p. 413 - 419
反应条件
pyridine; zinc(II) chloride 1.) dichloromethane, reflux, 2 h, 2.) dichloromethane, 5.5 h; Yield given. Multistep reaction;
参考文献
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, , vol. 30, # 3 p. 343 - 344
反应条件
in water; dimethyl sulfoxide T=37°C; pH=7.4; KineticsProduct distribution; Further Variations:pH-values;
参考文献
Chemical Research in Toxicology, , vol. 14, # 9 p. 1170 - 1176
反应条件
bei nachfolgender Oxydation mit Jod in Alkohol;
参考文献
Chemische Berichte, , vol. 45, p. 2194
反应条件
beim Erhitzen auf den Schmelzpunkt;
参考文献
Chemische Berichte, , vol. 45, p. 2194
参考文献
Weller et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1104
反应条件
ammonia in ethylene glycol dimethyl ether T=0 - 100°C; P=2625.26 - 4500.45 Torr; 5.8 h;
参考文献
Pastre, Julio C.; Browne, Duncan L.; O'Brien, Matthew; Ley, Steven V.
Organic Process Research and Development, 2013 , vol. 17, # 9 p. 1183 - 1191
反应条件
1: 57 percent / PPA / 0.25 h / 145 °C 2: 94 percent / KOH, H2O2 / H2O; methanol / 0.5 h / Ambient temperature 3: 95 percent / fuming HNO3, conc. H2SO4 / 0.5 h / 0 °C 4: 93 percent / H2 / 10percent Pd/C / methanol View Scheme
参考文献
Girard; Atkinson; Belanger; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3220 - 3234
反应条件
1: 57 percent / PPA / 0.25 h / 145 °C 2: 94 percent / KOH, H2O2 / H2O; methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Girard; Atkinson; Belanger; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3220 - 3234
