Zoete, Vincent; Bailly, Fabrice; Catteau, Jean-Pierre; Bernier, Jean-Luc
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 20 p. 2983 - 2988
in dichloromethane under Ar atm. soln. CmNH2 in CH2Cl2 was treated with soln. acetic-formicanhydride in CH2Cl2 and stirred for 20 min; react. mixt. was washed with aq. Na2CO3 and water, dried over Na2SO4, concd. and chromed. on silica, solvent was removed in vacuo; elem. anal.;
in benzene to suspn. of Rh complex in C6H6 added dropwise soln. of CH3COOC(O)H in C6H6 at room temp. under N2, stirred for 2 h; filtered, washed with pentane, dried;
参考文献
Doyle, Gerald
Journal of Organometallic Chemistry, 1982 , vol. 224, # 4 p. 355 - 362
