4'-叔丁基-2,2-二甲基苯丙酮合成路线 (共 14 条)
反应条件
1,4-diaza-bicyclo[2.2.2]octane in dimethyl sulfoxide T=35 - 40°C; 47 h; Irradiation;
参考文献
Russell, Glen A.; Chen, Ping; Kim, Byeong Hyo; Rajaratnam, Ragine
Journal of the American Chemical Society, 1997 , vol. 119, # 38 p. 8795 - 8801
反应条件
aluminium trichloride; benzene T=0°C;
参考文献
Grundy et al.
Journal of the Chemical Society, 1952 , p. 4136
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Pearson
Journal of the American Chemical Society, 1950 , vol. 72, p. 4169
反应条件
aluminium trichloride in benzene P=9375.7 Torr; 3 h; Ambient temperature; Yield given;
参考文献
Farcasiu, D.; Schlosberg, R. H.
Journal of Organic Chemistry, 1982 , vol. 47, # 1 p. 151 - 152
反应条件
etheric solution anschliessendes Behandeln mit Eis und wss. HCl;
参考文献
Pearson
Journal of the American Chemical Society, 1950 , vol. 72, p. 4169
反应条件
copper(l) chloride in diethyl ether 20 h; Ambient temperature;
参考文献
Eichin, Karl-Heinz; Beckhaus, Hans-Dieter; Hellmann, Siegried; Fritz, Hans; Peters, Eva-Maria; et al.
Chemische Berichte, 1983 , vol. 116, # 5 p. 1787 - 1821
反应条件
1: AlCl3 2: AlCl3 View Scheme
参考文献
Rothstein; Saville
Journal of the Chemical Society, 1949 , p. 1950,1953
反应条件
magnesium 1.) ether, 2.) ether, -15 deg C; Multistep reaction;
参考文献
Tsuji; Fujio; Tsuno
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 3 p. 856 - 866
反应条件
in tetrahydrofuran a) -84 deg C, 1h, b) room temperature, 1 h;
参考文献
McMahon, Kevin; Arnold, Donald R.
Canadian Journal of Chemistry, 1993 , vol. 71, # 4 p. 450 - 468
反应条件
in tetrahydrofuran a) -84 deg C, 1h, b) room temperature, 1 h;
参考文献
McMahon, Kevin; Arnold, Donald R.
Canadian Journal of Chemistry, 1993 , vol. 71, # 4 p. 450 - 468
反应条件
aluminium trichloride
参考文献
Rothstein; Saville
Journal of the Chemical Society, 1949 , p. 1950,1953