1,1-二氯-3,3-二甲基-2-丁酮合成路线 (共 16 条)
反应条件
1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione in acetonitrile T=20°C; 0.75 h; Inert atmosphere;
参考文献
Chen, Zizhan; Zhou, Bin; Cai, Huihua; Zhu, Wei; Zou, Xinzhuo
Green Chemistry, 2009 , vol. 11, # 2 p. 275 - 278
反应条件
chlorine; hydrogenchloride T=150°C; Heating / reflux;
参考文献
US2004/24256 A1, ;
Page 3 ;
反应条件
1: NCS / CCl4 2: H3O(1+) View Scheme
参考文献
Tetrahedron, , vol. 48, # 35 p. 7345 - 7362
反应条件
silver tetrafluoroborate in diethyl ether 5 h; Ambient temperature;
参考文献
Chemische Berichte, , vol. 117, # 6 p. 2193 - 2204
反应条件
1: 23 percent / PCl5 / 8 h / Heating 2: 51 percent / 90percent 3-Cl-C6H4-CO-OOH / CH2Cl2 / Heating 3: 3 percent Chromat. / AgBF4 / diethyl ether / 5 h / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 117, # 6 p. 2193 - 2204
反应条件
1: 51 percent / 90percent 3-Cl-C6H4-CO-OOH / CH2Cl2 / Heating 2: 3 percent Chromat. / AgBF4 / diethyl ether / 5 h / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 117, # 6 p. 2193 - 2204
参考文献
Tetrahedron, , vol. 48, # 35 p. 7345 - 7362
反应条件
beim Chlorieren in der Dampfphase;
参考文献
Journal of Organic Chemistry, , vol. 11, p. 785
Journal of the American Chemical Society, , vol. 55, p. 2511
Chimica e l'Industria (Milan, Italy), , vol. 24, p. 197
Chem. Zentralbl., , vol. 114, # I p. 1659
反应条件
chlorine in tetrachloromethane 1 h; Irradiation;
参考文献
Journal of Structural Chemistry, , vol. 54, # 3 p. 505 - 514
Zh. Strukt. Khim., , vol. 54, # 3 p. 453 - 462,10
参考文献
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, , vol. 278, p. 929 - 931