2-(2,4-二羟基苯基)-2H-苯并噻唑合成路线 （共 13 条）
反应条件
boron tribromide in dichloromethane; chloroform
24 h; Ambient temperature;
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1663 - 1673
反应条件
boron tribromide in dichloromethane
2 h; Ambient temperature;
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1663 - 1673
反应条件
boron tribromide in dichloromethane
72 h; Ambient temperature;
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1663 - 1673
反应条件
sodium hydroxide; zinc
参考文献
Elbs
Journal fuer Praktische Chemie (Leipzig), 1924 , vol. <2>108, p. 223
反应条件
1: 11.3 g / NaOH / 4 h / -5 - 5 °C
2: 92 percent / thiourea dioxide, 4N NaOH / ethanol / 80 °C
3: 91 percent / BBr3 / CH2Cl2 / 2 h / Ambient temperature
View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1663 - 1673
反应条件
1: 11.3 g / NaOH / 4 h / -5 - 5 °C
2: 92 percent / thiourea dioxide, 4N NaOH / ethanol / 80 °C
3: 91 percent / BBr3 / CH2Cl2 / 2 h / Ambient temperature
View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1663 - 1673
反应条件
1: 49 percent / acetic acid / Ambient temperature
2: 82 percent / 4N NaOH, thiourea dioxide / ethanol / 0.5 h / 80 °C
3: 96 percent / BBr3 / CH2Cl2; CHCl3 / 24 h / Ambient temperature
View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1663 - 1673
反应条件
1: 49 percent / acetic acid / Ambient temperature
2: 82 percent / 4N NaOH, thiourea dioxide / ethanol / 0.5 h / 80 °C
3: 96 percent / BBr3 / CH2Cl2; CHCl3 / 24 h / Ambient temperature
View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1663 - 1673
反应条件
1: 1) conc. HCl, NaNO2; 2) NaHCO3 / 1) water; 2) water, 0 deg C, 2 h
2: Zn, 2 N NaOH / H2O / 16 h
View Scheme
参考文献
Li,S.; Gupta,A.; Vogl,O.
Monatshefte fuer Chemie, 1983 , vol. 114, p. 937
反应条件
1: 1) conc. HCl, NaNO2; 2) NaHCO3 / 1) water; 2) water, 0 deg C, 2 h
2: Zn, 2 N NaOH / H2O / 16 h
View Scheme
参考文献
Li,S.; Gupta,A.; Vogl,O.
Monatshefte fuer Chemie, 1983 , vol. 114, p. 937
