1,1,3,3-四溴丙酮合成路线 （共 15 条）
反应条件
hydrogen bromide; bromine in water Bromination; 240 h;
参考文献
Kim; Hoffmann
European Journal of Organic Chemistry, 2000 , # 12 p. 2195 - 2201
参考文献
DE98009 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, V,711
参考文献
Chem. Zentralbl., , vol. 70, # I p. 596
DE98009 ;
参考文献
Arkiv foer Kemi, , vol. 21, p. 503,504
参考文献
Lederer
Patent: DE98009 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, V,711
反应条件
sodium hydrogencarbonate
参考文献
Rappe,C.; Andersson,K.
Acta Chemica Scandinavica (1947-1973), 1969 , vol. 23, p. 2839 - 2847
反应条件
zinc copper; pentacarbonyliron(0)
1.) THF, PhH, 2.) NH4Cl, MeOH; Yield given. Multistep reaction;
参考文献
Monti,S.A.; Harless,J.M.
Journal of the American Chemical Society, 1977 , vol. 99, # 8 p. 2690 - 2694
反应条件
silver; copper; ammonium chloride; zinc
1.) THF, 20 deg C, 12 h; 2.) CH3OH, 20 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Sato, T.; Noyori, R.
Tetrahedron Letters, 1980 , vol. 21, p. 2535 - 2538
反应条件
1: With boron triethoxide; bromine; zinc in tetrahydrofuran
T=80°C; 1.5 h;
2: With copper; ammonium chloride; zinc in methanol
T=20°C; 3 h; Further stages.;
参考文献
Hodgson, David M.; Paruch, Edyta
Tetrahedron, 2004 , vol. 60, # 24 p. 5185 - 5199
反应条件
bromide; copper; zinc
1.) furan, benzene, 60 deg C, 5 h, 2.) methanol, NH4Cl, 25 deg C, 1 h; Yield given;
参考文献
Sato, T.; Watanabe, M.; Noyori, R.
Heterocycles, 1980 , vol. 14, # 6 p. 761 - 764
