1,1,3,3-四溴丙酮合成路线 （共 15 条）
反应条件
boron triethoxide; zinc in tetrahydrofuran
19 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Li, Jing; Van Belkum, Marco J.; Vederas, John C.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 14 p. 4356 - 4363
反应条件
diethylzinc in toluene
T=-12 - 20°C; 18 h;
参考文献
Cramer, Nicolai; Laschat, Sabine; Baro, Angelika; Frey, Wolfgang
Synlett, 2003 , # 14 p. 2175 - 2177
反应条件
diethylzinc in toluene
T=-12 - 20°C; 18 h;
参考文献
Cramer, Nicolai; Laschat, Sabine; Baro, Angelika; Frey, Wolfgang
Synlett, 2003 , # 14 p. 2175 - 2177
反应条件
diethylzinc; copper; ammonium chloride; zinc
1) benzene, hexane, a) 0 deg C, 3 h, b) r.t., 19 h, 2) MeOH, r.t., 2.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mann, John; Barbosa, Luiz-Claudio de Almeida
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 7 p. 787 - 790
反应条件
copper; ammonium chloride; zinc
1) benzene, hexane, a) 0 deg C, 3 h, b) r.t., 19 h, 2) MeOH, r.t., 2.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mann, John; Barbosa, Luiz-Claudio de Almeida
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 7 p. 787 - 790
