3-甲基-1-壬烯-3-醇合成路线 （共 6 条）
反应条件
bis(acetylacetonate)oxovanadium; bis(trimethylsilyl)-peroxide in dichloromethane T=25°C; 24 h;
参考文献
Matsubara; Okazoe; Oshima; Takai; Nozaki
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 3 p. 844 - 849
反应条件
1: 1-bromo-hexane With lithium in diethyl ether T=20°C; 2 h; 2: methyl vinyl ketone in diethyl ether T=0°C;
参考文献
Koufaki, Maria; Calogeropoulou, Theodora; Rekka, Eleni; Chryselis, Michael; Papazafiri, Panagiota; Gaitanaki, Catherine; Makriyannis, Alexandros
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 23 p. 5209 - 5219
反应条件
in tetrahydrofuran 1.) -10 deg C to 0 deg C, 30 min, 2.) r.t., 2 h;
参考文献
Harnett, J. J.; Alcaraz, L.; Mioskowski, C.; Martel, J. P.; Gall, T. Le; et al.
Tetrahedron Letters, 1994 , vol. 35, # 13 p. 2009 - 2012
反应条件
hydrogen; ruthenium palladium
参考文献
Karavanov, A. N.; Gryaznov, V. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 8.1 p. 1593 - 1596
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 8 p. 1740 - 1745
反应条件
hydrogen; ruthenium palladium in propan-1-ol T=89.9°C; Rate constant;
参考文献
Karavanov, A. N.; Gryaznov, V. M.; Batyrev, I. G.; Olenina, E. G.
Russian Journal of Physical Chemistry, 1995 , vol. 69, # 5 p. 739 - 743
Zhurnal Fizicheskoi Khimii, 1995 , vol. 69, # 5 p. 816 - 821
反应条件
acetic acid in di-isopropyl ether
3 h; Heating;
参考文献
Koufaki, Maria; Calogeropoulou, Theodora; Rekka, Eleni; Chryselis, Michael; Papazafiri, Panagiota; Gaitanaki, Catherine; Makriyannis, Alexandros
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 23 p. 5209 - 5219
