1-(2-甲氧基苯基)-3-苯基-1-丙酮合成路线 (共 7 条)
反应条件
pyrrolidine; CataCXium POMetB; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl acetamide T=140°C; 4 h; Inert atmosphereMolecular sieve;
参考文献
Colbon, Paul; Ruan, Jiwu; Purdie, Mark; Xiao, Jianliang
Organic Letters, 2010 , vol. 12, # 16 p. 3670 - 3673
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; silica gel in benzene T=70°C; 18 h;
参考文献
Yasui, Shinro; Fujii, Masayuki; Ohno, Atsuyoshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 11 p. 4019 - 4026
反应条件
N-benzyl-N,N,N-triethylammonium chloride; palladium diacetate; sodium hydrogencarbonate in acetonitrile T=50°C; Mizoroki-Heck reaction; 1.5 h; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Krishna; Reddy, A. Gopi Krishna; Ramulu, B. Venkat; Mahendar; Satyanarayana
Synlett, 2012 , # 3 p. 375 - 380
反应条件
in tetrahydrofuran T=20°C; 8 h; Product distribution; Further Variations:Temperaturesreaction times;
参考文献
Nudelman; Garcia
Journal of Organic Chemistry, 2001 , vol. 66, # 4 p. 1387 - 1394
反应条件
(i) Cd, benzene, (ii) /BRN= 607605/; Multistep reaction;
参考文献
Hase,T.
Acta Chemica Scandinavica (1947-1973), 1968 , vol. 22, p. 2845 - 2850
反应条件
in tetrahydrofuran T=20°C; 8 h; Product distribution; Further Variations:reaction times;
参考文献
Nudelman; Garcia
Journal of Organic Chemistry, 2001 , vol. 66, # 4 p. 1387 - 1394
反应条件
boron trichloride in chloroform
参考文献
Hase,T.
Acta Chemica Scandinavica (1947-1973), 1968 , vol. 22, p. 2845 - 2850