1,2,11,12-四氯二十二氟十二烷合成路线 (共 5 条)
反应条件
acetic anhydride; zinc in dichloromethane T=40°C; 3 h; Inert atmosphere;
参考文献
Wlassics, Ivan; Tortelli, Vito
Collection of Czechoslovak Chemical Communications, 2008 , vol. 73, # 12 p. 1719 - 1728
反应条件
acetic anhydride; zinc in N,N-dimethyl-formamide T=40°C;
参考文献
Wlassics, Ivan; Tortelli, Vito
Collection of Czechoslovak Chemical Communications, 2008 , vol. 73, # 12 p. 1719 - 1728
反应条件
acetic anhydride; zinc in dichloromethane T=40°C; 10 h;
参考文献
Wlassics, Ivan; Tortelli, Vito
Collection of Czechoslovak Chemical Communications, 2008 , vol. 73, # 12 p. 1719 - 1728
反应条件
dichloromethane; acetic anhydride; zinc
参考文献
Knunyants,I.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1961 , p. 1361 - 1366
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 1462 - 1468
反应条件
1: Zn, Ac2O / acetic acid 2: aq. KMnO4 / acetone View Scheme
参考文献
Knunyants,I.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1961 , p. 1361 - 1366
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 1462 - 1468