2H-苯并吡喃-3-甲酸合成路线 (共 29 条)
参考文献
Taylor; Tomlinson
Journal of the Chemical Society, 1950 , p. 2724
反应条件
1: 90 percent / hydrogen / 10 percent Pd/C / ethanol / 2 h / Ambient temperature 2: 66 percent / LiAlH4 / diethyl ether / 4 h View Scheme
参考文献
Mouysset, Genevieve; Payard, Marc; Grassy, Gerard; Tronche, Pierre; Dabire, Hubert; et al.
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 539 - 544
反应条件
hydrogen; palladium on activated charcoal in ethanol 2 h; Ambient temperature;
参考文献
Mouysset, Genevieve; Payard, Marc; Grassy, Gerard; Tronche, Pierre; Dabire, Hubert; et al.
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 539 - 544
反应条件
1: With diphenyl phosphoryl azide in dichloromethane; triethylamine; toluene T=50°C; 1 h; 2: in dichloromethane; triethylamine; toluene T=85°C; Curtius rearrangement; 3 h; 3: With hydrogenchloride in dichloromethane; triethylamine; toluene 3 h; Heating; Further stages.;
参考文献
Alami, Mouad; Peyrat, Jean-Francois; Belachmi, Larbi; Brion, Jean-Daniel
European Journal of Organic Chemistry, 2001 , # 22 p. 4207 - 4212
反应条件
1: 90 percent / hydrogen / 10 percent Pd/C / ethanol / 2 h / Ambient temperature 2: thionyl chloride / cyclohexane / 6 h / Heating View Scheme
参考文献
Mouysset, Genevieve; Payard, Marc; Grassy, Gerard; Tronche, Pierre; Dabire, Hubert; et al.
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 539 - 544
反应条件
lithium aluminium tetrahydride in diethyl ether 4 h;
参考文献
Mouysset, Genevieve; Payard, Marc; Grassy, Gerard; Tronche, Pierre; Dabire, Hubert; et al.
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 539 - 544
反应条件
1: 90 percent / hydrogen / 10 percent Pd/C / ethanol / 2 h / Ambient temperature 2: 66 percent / LiAlH4 / diethyl ether / 4 h 3: 88 percent / thionyl chloride / CHCl3 / 10 h / Ambient temperature View Scheme
参考文献
Mouysset, Genevieve; Payard, Marc; Grassy, Gerard; Tronche, Pierre; Dabire, Hubert; et al.
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 539 - 544
反应条件
1: SOCl2 / benzene / 3 h / Heating
2: Et3N / benzene
View Scheme
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347
反应条件
1: SOCl2 / benzene / 3 h / Heating
2: Et3N / benzene
View Scheme
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347
反应条件
1: SOCl2 / benzene / 3 h / Heating
2: Et3N / benzene
View Scheme
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347