1,4-二氟-2-碘代苯合成路线 （共 10 条）
反应条件
N-iodo-succinimide; boron trifluoride T=0 - 5°C; 0.25 h;
参考文献
Prakash, G. K. Surya; Mathew, Thomas; Hoole, Dushyanthi; Esteves, Pierre M.; Wang, Qi; Rasul, Golam; Olah, George A.
Journal of the American Chemical Society, 2004 , vol. 126, # 48 p. 15770 - 15776
反应条件
Diazotization.Behandlung der Diazoniumsalz-Loesung mit KI;
反应条件
1: Cu / 200 °C 2: HNO3 View Scheme
参考文献
Namkung,M.J.; Fletcher,T.L.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2569 - 2575
反应条件
1: Cu / 200 °C 2: HNO3 3: phosphorus, aq. HI View Scheme
参考文献
Namkung,M.J.; Fletcher,T.L.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2569 - 2575
反应条件
1: Cu / 200 °C 2: HNO3 3: SnCl2*2H2O, aq. HCl 4: (i) NaNO2, aq. HBF4, (ii) (thermolysis) 5: HNO3 View Scheme
参考文献
Namkung,M.J.; Fletcher,T.L.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2569 - 2575
参考文献
Namkung,M.J.; Fletcher,T.L.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2569 - 2575
反应条件
1: 66 percent / LDA; I2 / tetrahydrofuran; hexane / -75 °C 2: 18 percent Chromat. / LDA / tetrahydrofuran; hexane / -75 °C 3: 97 percent / tBuOK; H2O / diethyl ether / 2 h / 25 °C View Scheme
参考文献
Rausis, Thierry; Schlosser, Manfred
European Journal of Organic Chemistry, 2002 , # 19 p. 3351 - 3358
反应条件
1: Cu / 200 °C
2: HNO3
3: SnCl2*2H2O, aq. HCl
4: (i) NaNO2, aq. HBF4, (ii) (thermolysis)
5: HNO3
6: SnCl2*2H2O, aq. HCl
7: (i) NaNO2, aq. HBF4, (ii) (thermolysis)
View Scheme
参考文献
Namkung,M.J.; Fletcher,T.L.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2569 - 2575
反应条件
1: Cu / 200 °C
2: HNO3
3: SnCl2*2H2O, aq. HCl
4: (i) NaNO2, aq. HBF4, (ii) (thermolysis)
5: HNO3
6: SnCl2*2H2O, aq. HCl
View Scheme
参考文献
Namkung,M.J.; Fletcher,T.L.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2569 - 2575
反应条件
1: Cu / 200 °C
2: HNO3
3: SnCl2*2H2O, aq. HCl
4: (i) NaNO2, aq. HBF4, (ii) (thermolysis)
View Scheme
参考文献
Namkung,M.J.; Fletcher,T.L.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2569 - 2575
