3,7-二甲基-6-辛烯-3-醇合成路线 (共 24 条)
反应条件
oxygen; 5-ethyl-3-methyllumiflavin perchlorate; hydrazine hydrate; phenol in acetonitrile T=25 - 30°C; 5 h; chemoselective reaction;
参考文献
Imada, Yasushi; Iida, Hiroki; Kitagawa, Takahiro; Naota, Takeshi
Chemistry - A European Journal, 2011 , vol. 17, # 21 p. 5908 - 5920
反应条件
anhydrous ammonium carbonate in water; hydrogen
参考文献
Nissan Chemical Industries, Ltd.
Patent: US4188498 A1, 1980 ;
反应条件
in diethyl ether Heating;
参考文献
Ho, Tse-Lok
Synthetic Communications, 1982 , vol. 12, # 1 p. 53 - 56
反应条件
n-butyllithium; ammonium chloride in tetrahydrofuran
反应条件
FeCl3·6H2O; hydrazine hydrate in ethanol T=80°C; 36 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 8 p. 1437 - 1442
反应条件
hydrogen; Lindlar's catalyst in octane T=20°C; P=760 Torr; other solvents (ethanol, acetic acid), other catalyst (2.8percent Pd/C); dependence of reaction rate; Product distribution;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 46, # 5 p. 1258 - 1261
参考文献
Nissan Chemical Industries, Ltd.
Patent: US4188498 A1, 1980 ;
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile T=0°C; 0.5 h; Product distribution;
参考文献
Masaki, Yukio; Iwata, Ikuhiro; Mukai, Isao; Oda, Hirohisa; Nagashima, Hiromu
Chemistry Letters, 1989 , p. 659 - 662
反应条件
1: With mercury(II) diacetate in tetrahydrofuran; water T=22°C; 2.1 h; 2: With sodium hydroxide; sodium tetrahydroborate in tetrahydrofuran; water 0.5 h;
参考文献
Journal of Chemical Ecology, , vol. 28, # 12 p. 2527 - 2539
反应条件
lithium; ethylamine T=-78°C;
参考文献
Tetrahedron, , vol. 33, p. 579 - 580