反应条件
H2SO4 in sulfuric acid treatment of digermane deriv. with concd. H2SO4 for 24 min at room temp., addn. of NH4Cl, cooling to 0°C, stirring for 30 min; Triplett K., Curtis M.D., J. Organomet. Chem., 1976, 107, 23-32; separating ppt., recrystn. (pentane), sublimation at 40°C and 0.1Torr, NMR;
参考文献
Hoelbling, Margit; Masters, Sarah L.; Flock, Michaela; Baumgartner, Judith; Hassler, Karl; Robertson, Heather E.; Wann, Derek A.
Inorganic Chemistry, 2008 , vol. 47, # 8 p. 3023 - 3033
