反应条件
1: PCl5 2: 1.) Me3SnLi / 1.) THF, -78 deg C, 1 h; room temperature, 1 h, 2.) Et2O, room temperature, 15 min 3: 68 percent / HCl / tetrahydrofuran / 0.25 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 16 p. 2283 - 2288