water in tetrahydrofuran treatment od reaction mixt. in THF with excess EtMgBr, hydrolysis; extn. (ether), drying over Na2SO4; identification of individual compds.;
参考文献
Riviere, P.; Castel, A.; Abdennadher, C.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 82, # 1-4 p. 181 - 194
hydrogenchloride in tetrahydrofuran treatment od reaction mixt. in THF with HCl soln., stirring (15 min); org. phase sepn., drying over Na2SO4 (24 h), soln. concn.; identification of individual compds.;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 82, # 1-4 p. 181 - 194
