反应条件
hydrogenchloride in toluene
inert atmosphere; addn. of org. compd. soln. to soln. of Ge-compd. at -78°C, keeping at same temp. for 2 h, soln. allowing to stay at room temp. for 12 h, soln. hydrolysis (HCl); soln. decanting, drying (Na2SO4), soln. concn. (reduced pressure); (1)H-NMR spectroscopy;
参考文献
Riviere, P.; Castel, A.; Desor, D.; Abdennadher, C.
Journal of Organometallic Chemistry, 1993 , vol. 443, # 1 p. 51 - 60
