反应条件
HCl in methanol
MeOH soln. of thioacetic acid added to MeOH suspn. of (CH3)2SnO, stirredfor 30 min at 18°C, MeOH soln. of HCl added, stirred for 4 h; solvent evapd. under reduced pressure, residue extd. with CHCl3, filtered, solvent evapd. under reduced pressure, dried under vac. for 2 h, recrystd. from CHCl3; elem. anal.;
参考文献
Chaturvedi, Jyotsna; Bhattacharya, Subrato; Nethaji
Dalton Transactions, 2009 , # 38 p. 8018 - 8024
