1: With lithium hexamethyldisilazane in tetrahydrofuran T=-78°C; 0.583333 h; 2: With TFETFA in tetrahydrofuran T=-78°C; 0.166667 h; 3: With triethylamine; Methanesulfonyl azide in water; acetonitrile T=20°C; 13.5 h; Further stages.;

暂无反应条件数据

1: thionyl chloride / benzene / 1 h / Heating 2: triethylamine / diethyl ether / 16 h / 20 °C View Scheme

1: aq. KOH / methanol 2: SOCl2 3: diethyl ether / 0 °C View Scheme

1: 910 mg / silver(I) acetate / dioxane; H2O / 1.5 h / Heating 2: thionyl chloride / benzene / 1 h / Heating View Scheme

1: 910 mg / silver(I) acetate / dioxane; H2O / 1.5 h / Heating 2: thionyl chloride / benzene / 1 h / Heating 3: triethylamine / diethyl ether / 1 h / 20 °C View Scheme