4,4-二甲基-2-环戊烯-1-酮合成路线 (共 40 条)
参考文献
Journal of the American Chemical Society, , vol. 101, # 14 p. 3961 - 3963
反应条件
1: HgSO4, aq. H2SO4 2: aq. KOH View Scheme
参考文献
Journal of the American Chemical Society, , vol. 98, # 20 p. 6317 - 6321
反应条件
1: CrO3, H2SO4 2: 600 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 101, # 14 p. 3961 - 3963
反应条件
1: CF3CO2H 2: polyphosphoric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 93, p. 5513 - 5520
反应条件
lithium carbonate; lithium bromide in N,N-dimethyl-formamide
参考文献
Journal of Organic Chemistry, , vol. 44, p. 689 - 691
反应条件
1: 79 percent / sodium / toluene / 28 h 2: 87 percent / 85 percent phosphoric acid / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 8 p. 1445 - 1451
反应条件
1: 97 percent / H2SO4, H2O 2: 92 percent / H2SO4 / toluene 3: 79 percent / sodium / toluene / 28 h 4: 87 percent / 85 percent phosphoric acid / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 8 p. 1445 - 1451
反应条件
1: 1.) O3/O2, 2.) PPh3 / 1.) MeOH, CH2Cl2, -60 deg C, 2.) RT, 5 h 2: 70 percent / 1M KOH / methanol / 4 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 10 p. 1683 - 1686
反应条件
1: 95 percent / Hg(OAc)2 / 170 - 175 °C / in sealed tube 2: 1.) O3/O2, 2.) PPh3 / 1.) MeOH, CH2Cl2, -60 deg C, 2.) RT, 5 h 3: 70 percent / 1M KOH / methanol / 4 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 10 p. 1683 - 1686
参考文献
Annales Academiae Scientiarum Fennicae, Series A, , vol. 49, # 1 p. 93,106